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Friday, June 17, 2011

Investigating N-methoxy-N′-aryl ureas in oxidative C–H olefination reactio: an unexpected oxidation behaviour


Abstract:
Herein, we report a urea derived directing group for mild and highly selective oxidative C–H bond olefination. Subsequent intramolecular Michael addition affords dihydroquinazolinones in good yields. The N–O bond of the urea substrate exhibits superior oxidative behaviour compared to a variety of other external oxidants.
Graphical abstract: Investigating N-methoxy-N′-aryl ureas in oxidative C–H olefination reactions: an unexpected oxidation behaviour
Frank Glorius, Org. Biomol. Chem, 2011, 9, 4736

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